N-(2-Aminoethyl)-5-(dimethylamino)naphthalene-1-sulfonamide

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N-(2-Amino­ethyl)-5-(dimethyl­amino)naphthalene-1-sulfonamide

In the title compound, C(14)H(19)N(3)O(2)S, the N atom of the dimethyl-amino group and the S atom are displaced by 0.078 (2) and 0.084 (2) Å, respectively, from the naphthalene ring plane. The 2-amino-ethyl group has a coiled conformation with an N-C-C-NH(2) torsion angle of 53.6 (4)°. In the crystal structure, inter-molecular N-H⋯N and weak C-H⋯O hydrogen bonds link mol-ecules into chains alon...

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N-(5-Bromo-2-chloro­benz­yl)-N-cyclo­propyl­naphthalene-2-sulfonamide

In the title compound, C(20)H(17)BrClNO(2)S, the dihedral angle between the benzene ring and the naphthalene plane is 8.95 (8)°. The crystal packing is stabilized by weak inter-molecular C-H⋯O, C-H⋯Cl and π-π [centroid-centroid distance = 3.8782 (16) Å] inter-actions.

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N-Cyclo­dodecyl-5-(dimethyl­amino)­naphthalene-1-sulfonamide

The molecule of the title compound, C(24)H(36)N(2)O(2)S, displays a U-shaped conformation. The prominent inter-molecular inter-actions are N-H⋯O hydrogen bonds, resulting in the formation of dimers. Additional C-H⋯π contacts involving one of the methyl-ene groups of the macrocycle and the naphthalene rings of a neighbouring mol-ecule stabilize the packing structure. In the crystal structure, th...

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N-Benzyl-5-(dimethyl­amino)­naphthalene-1-sulfonamide

The structure of the title compound, C(19)H(20)N(2)O(2)S, displays inter-molecular N-H⋯O hydrogen bonding, which generates inversion dimers. There is no π-π stacking in the crystal structure. The dihedral angle between the phenyl ring and naphthalene ring system is 59.16 (11)°.

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N-Benzyl­pyridine-2-sulfonamide

The title compound, C(12)H(12)N(2)O(2)S, was obtained by the reaction of 2-mercaptopyridine and benzyl-amine. The dihedral angle between the benzene and pyridine rings is 75.75 (9)°. In the crystal, mol-ecules are linked into chains along the c axis by N-H⋯O and N-H⋯N hydrogen bonds; the chains are cross-linked into a two-dimensional network parallel to the bc plane via C-H⋯O hydrogen bonds.

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2009

ISSN: 1600-5368

DOI: 10.1107/s160053680901962x